Patra, Nitish Kumar and Chhatria, Paramananda (2015) Electrochemical Exfoliation of Graphene and its Characterisation. BTech thesis.
A green approach is reported for the production of few layered graphenes (FLGs) via electrochemical route utilising the benefits of anodic exfoliation process, wherein electrochemical intercalation of nitrate ions into pyrolytic graphite resulted in electrochemical exfoliation of nitrate ions-intercalated graphite electrode. The role of applied potential in intercalation and concentrations of nitric acid are well defining factors in controlling the number of layers in FLGs. The success of this approach was confirmed by FTIR, wherein smaller particles of intercalated graphite led to broader peaks due to increased interaction with light wave. The SEM images showed several layers of graphene stacked together and slightly twisted at edges. An increased exfoliation in intercalated graphite was revealed by XRD patterns. Desirable conductive properties of the FLGs synthesised makes it a viable option for utility as conductive ink.
|Item Type:||Thesis (BTech)|
|Uncontrolled Keywords:||Pyrolytic Graphite, Exfoliation, Intercalation, Few layered graphene, Graphene Oxide|
|Subjects:||Engineering and Technology > Metallurgical and Materials Science > Nanotechnology > Electrochemical Systhesis|
|Divisions:||Engineering and Technology > Department of Metallurgical and Materials Engineering|
|Deposited By:||Mr. Sanat Kumar Behera|
|Deposited On:||19 May 2016 20:03|
|Last Modified:||19 May 2016 20:03|
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